Instruments

 

Environmental Scanning

 Electron Microscope

 

 

FEI Quanta 400 (ESEM) – completely digital in two dimensions (d=3.2nm) with integrated Oxford INCA Energy 400  EDS w\GSR(Feature) (automated imaging, elemental and morphometric analyses)

 

The Quanta 400 with the integrated Oxford INCA EDS system provides a means by which completely digital imaging can be performed on objects from low pressures (10-6 torr to quite high pressures (20 torr) in hydrated condition or in other gasses in which imaging can be performed.  This variable pressure instrument provides an opportunity to capture dynamic imaging (as movies!) on specimens from the physical to the biological.  The EDS system includes almost every software module marketed by Oxford including its automated modules, 'Automate' and 'Feature'.  Automate permits automation of normal x-ray acquisition methods including mixes of Analysis, Point & ID and Mapping with or without 'Montage'.  Feature provides morphometric and elemental analyses based on grayscale identification of features of interest in multiple and/or large specimens.  16 circular stubs with particulate specimens finished in about 8 hours providing a complete data set of both morphometric and elemental analyses for each particle detected by the criteria established by the user.  Particles can range from less than 10 to several hundred micrometers, and detection can extend to as low as 1 micrometer.  'Feature' and 'Automate' provide the capability to perform large area elemental mapping (95 x 95mm) of fresh sawed geologic or metallurgic specimens.   The Gun Shot Residue (GSR) module integrates nicely with the Forensic Concentration in the Chemistry Department.

 

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